Here are some things I've given recently:
Fireplace Stuff. This came with my house and after not using it for a year, I am sure I can part with it.
Chocolate Chip Cookies. My addiction. Offering these on freecycle was a big hit! I met some cool people. These two nice brothers came over by bicycle and had cookies on my porch. (And took a bag home with them.) They tipped me off to the free garden soil at the ecolgy center!
Bike shorts. By coincidence the person who asked for them was the person who gave me the pantyhose!